Ethylvanillin → HCID 68458774, compound

HRID 502371Notes

Reaction equation

HRID 502371 reaction equation
[CH3:1][C:2]1[CH:3]=[N:4][CH:5]=[C:6]([CH:16]=1)[C:7]([NH:9][CH:10]1[CH2:15][CH2:14][NH:13][CH2:12][CH2:11]1)=[O:8].[CH2:17]([O:19][C:20]1[CH:21]=[C:22]([CH:25]=[CH:26][C:27]=1[OH:28])[CH:23]=O)[CH3:18]>>[CH2:17]([O:19][C:20]1[CH:21]=[C:22]([CH:25]=[CH:26][C:27]=1[OH:28])[CH2:23][N:13]1[CH2:12][CH2:11][CH:10]([NH:9][C:7](=[O:8])[C:6]2[CH:16]=[C:2]([CH3:1])[CH:3]=[N:4][CH:5]=2)[CH2:15][CH2:14]1)[CH3:18]

Participants

3

Reactant 2

HCID 8467EthylvanillinHCID 655621085-Methyl-N-(piperidin-4-yl)-nicotinamide

Product 1

HCID 68458774HCID 68458774, compoundYield 100%

Procedure

The title compound (37 mg, 100%) was prepared analogously to example 30 from 5-methyl-N-(piperidin-4-yl)-nicotinamide and 3-ethoxy-4-hydroxy-benzaldehyde. MS: 370.5 (MH+).

Sources & evidence

ORD record
ord-8b794f83f60844de909f2355ca0972ba
Source dataset
uspto-grants-2010_08
Patent number
US07772253B2

Reaction notes

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