HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Pyridine → Pyridinium, 1-(2-ethoxy-2-oxoethyl)-, bromide (1:1)
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Pyridine | HCID 1049 | — |
| Edukt | Ethyl bromoacetate | HCID 7748 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | Pyridinium, 1-(2-ethoxy-2-oxoethyl)-, bromide (1:1) | HCID 87028 | — |
Reaktionsschritte
A mixture of pyridine (3 g, 38 mmol) and ethyl bromoacetate (6.3 g, 38 mmol) in 30 ml of ethyl acetate was stirred for 12 h. The precipitate formed was isolated by filtration and washed with diethyl ether (30 ml), to give, after drying, 7 g of 1-ethoxycarbonylmethylpyridinium bromide 5.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07776107B2 |
| Quelldatensatz | uspto-grants-2010_08 |
| ORD ID | ord-c170f83e431a458ea4685534f1fe1bf2 |
| Quellennotiz | uspto-grants-2010_08 |