HRID502474

反应详情

EQUATION

反应方程式

HRID 502474 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of pyridine (3 g, 38 mmol) and ethyl bromoacetate (6.3 g, 38 mmol) in 30 ml of ethyl acetate was stirred for 12 h. The precipitate formed was isolated by filtration and washed with diethyl ether (30 ml), to give, after drying, 7 g of 1-ethoxycarbonylmethylpyridinium bromide 5.

WORKUP

后处理

  1. customThe precipitate formed
  2. customwas isolated by filtration
  3. washwashed with diethyl ether (30 ml)
  4. customto give
  5. customafter drying