Benzenamine hydrochloride (1:1) → HCID 86611051, compound

Participants

Reaction Steps

To the crude crude 2-(5-buta-1,3-dienyl-2-iodo-4-methyl-phenoxy)-3-dimethylamino-acrylonitrile of step 3 was added aniline hydrochloride (2.54 g, 19.59 mmol) and ethanol (25 mL). The mixture was heated to reflux for 16 hours under nitrogen atmosphere. The mixture was cooled and concentrated under reduced pressure to yield crude 2-(5-buta-1,3-dienyl-2-iodo-4-methyl-phenoxy)-3-phenylamino-acrylonitrile, which was used in the same flask directly in the following step.

Provenance & Evidence