tert-Butyl carbazate → HCID 68468108, compound

HRID 502962Notes

Reaction equation

HRID 502962 reaction equation
Cl.[NH:2]([C:9]1([C:14]([OH:16])=O)[CH2:13][CH2:12][CH2:11][CH2:10]1)[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.O.N1(O)C2C=CC=CC=2N=N1.[NH:28]([C:30]([O:32][C:33]([CH3:36])([CH3:35])[CH3:34])=[O:31])[NH2:29].C(N(C(C)C)CC)C>CN(C=O)C>[NH:2]([C:9]1([C:14]([NH:29][NH:28][C:30]([O:32][C:33]([CH3:36])([CH3:35])[CH3:34])=[O:31])=[O:16])[CH2:10][CH2:11][CH2:12][CH2:13]1)[C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=1

Participants

6

Reactant 4

HCID 70091tert-Butyl carbazateHCID 521913N,N-Diethyl-2-propanamineHCID 27960291-Hydroxybenzotriazole hydrateHCID 68468741HCID 68468741, compound

Product 1

HCID 68468108HCID 68468108, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

1-Anilinocyclopentanecarboxylic acid hydrochloride and N-[3-(dimethylaminopropyl)]-N′-ethylcarbodiimide hydrochloride, 1H-1,2,3-benzotriazol-1-ol hydrate, tert-butyl hydrazinecarboxylate, N,N-diethylisopropylamine were stirred in DMF at room temperature to obtain tert-butyl 2-[(1-anilinocyclopentyl)carbonyl]hydrazinecarboxylate.

Sources & evidence

ORD record
ord-13122f4574d74bf68d97593eec6b0f5d
Source dataset
uspto-grants-2010_08
Patent number
US07776897B2

Reaction notes

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