HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13683465, compound → HCID 68468755, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13683465 | HCID 13683465 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Catalyst | Methyltriphenyliphosphonium bromide | HCID 74505 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 68468755 | HCID 68468755 | — |
Reaction Steps
After methyltriphenylphosphonium bromide and n-butyllithium were reacted in THF, a THF solution of tert-butyl 2,2-dimethyl-3-oxo-3-phenylpropanoate was added thereto and the whole was reacted under heating to obtain tert-butyl 2,2-dimethyl-3-phenylbut-3-enoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07776897B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-ed02ba113d154f4d992de851b6f3065f |
| Source note | uspto-grants-2010_08 |