Triethylamine → HCID 40718563, compound

HRID 502972Notes

Reaction equation

HRID 502972 reaction equation
Cl.[NH2:2][CH2:3][CH2:4][NH:5][C:6](=[O:14])[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[Cl:13].C(N(CC)CC)C.[CH3:22][S:23](Cl)(=[O:25])=[O:24]>ClCCl>[Cl:13][C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=1[C:6]([NH:5][CH2:4][CH2:3][NH:2][S:23]([CH3:22])(=[O:25])=[O:24])=[O:14]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 31297Methanesulfonyl chlorideHCID 1302801194319-83-2

Product 1

HCID 40718563HCID 40718563, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

N-(2-Aminoethyl)-2-chlorobenzamide hydrochloride was suspended in dichloromethane and stirred with triethylamine and methanesulfonyl chloride to obtain 2-chloro-N-{2-[(methylsulfonyl)amino]ethyl}benzamide.

Sources & evidence

ORD record
ord-d08f216f64eb41e9910a9bdb55f2bd79
Source dataset
uspto-grants-2010_08
Patent number
US07776897B2

Reaction notes

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