HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → 2-[5-(2-Chlorophenyl)-4-methyl-1,2,4-triazol-3-yl]-2-methylpropanal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | Ethyl 2-[5-(2-chlorophenyl)-4-methyl-1,2,4-triazol-3-yl]-2-methylpropanoate | HCID 68468476 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2-[5-(2-Chlorophenyl)-4-methyl-1,2,4-triazol-3-yl]-2-methylpropanal | HCID 86616223 | — |
Reaction Steps
Ethyl 2-[5-(2-chlorophenyl)-4-methyl-1,2,4-triazol-3-yl]-2-methylpropanoate was reacted with diisobutylaluminum hydride in toluene at −78° C. to obtain 2-[5-(2-chlorophenyl)-4-methyl-1,2,4-triazol-3-yl]-2-methylpropanal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07776897B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-279c9d7552724430a884f17002e5db37 |
| Source note | uspto-grants-2010_08 |