Methylamine → HCID 68465430, compound

Participants

Reaction Steps

Methyl 4-[5-(1-anilino-1-methylethyl)-4-methyl-4H-1,2,4-triazol-3-yl}benzoate (300 mg) was dissolved in methanol (1 ml) and then methylamine (30% methanol solution, 886.3 mg) was added thereto, followed by stirring at room temperature overnight. The resulting precipitate was collected by filtration to obtain 349 mg of 4-[5-(1-anilino-1-methylethyl)-4-methyl-4H-1,2,4-triazol-3-yl}benzamide (white crystals).

Provenance & Evidence