Acetic Anhydride → HCID 68471202, compound

Participants

Reaction Steps

Acetic anhydride (37 μl) was added to a pyridine solution (1 ml) of 4-[5-(1-anilino-1-methylethyl)-4-methyl-4H-1,2,4-triazol-3-yl}phenol (60 mg), followed by stirring for 3 hours. After most of acetic anhydride and pyridine was removed by evaporation under reduced pressure, the residue was purified by thin layer chromatography (chloroform:methanol=9:1) to obtain 40 mg of 4-[5-(1-anilino-1-methylethyl)-4-methyl-4H-1,2,4-triazol-3-yl}phenyl acetate (white crystals).

Provenance & Evidence