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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 503177Generated: October 30, 2026

HCID 22260898, compound → HCID 22260893, compound

https://huagongshe.com/reaction/503177

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22260898HCID 22260898—
CatalystHCID 178418406HCID 178418406—
SolventDichloromethaneHCID 6344—
ProductHCID 22260893HCID 2226089395.3%

Reaction Steps

To a solution of 1.72 g of (3-bromo-6-fluoro-2-methoxy-phenyl)-naphthalen-2-yl-methanol in 34.4 ml methylene chloride was added 5.16 g of activated manganese dioxide, followed by stirring at room temperature for 17 hours. Then, the manganese dioxide was filtered off through Celite. The solvent was removed by distillation, to give 1.63 g of the title compound as a yellow oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07776890B2
Source datasetuspto-grants-2010_08
ORD IDord-bbdb8fa6ec564c82abb11b6440bc7ef4
Source noteuspto-grants-2010_08