HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22260898, compound → HCID 22260893, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22260898 | HCID 22260898 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22260893 | HCID 22260893 | 95.3% |
Reaction Steps
To a solution of 1.72 g of (3-bromo-6-fluoro-2-methoxy-phenyl)-naphthalen-2-yl-methanol in 34.4 ml methylene chloride was added 5.16 g of activated manganese dioxide, followed by stirring at room temperature for 17 hours. Then, the manganese dioxide was filtered off through Celite. The solvent was removed by distillation, to give 1.63 g of the title compound as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07776890B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-bbdb8fa6ec564c82abb11b6440bc7ef4 |
| Source note | uspto-grants-2010_08 |