HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 18412535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 18412489 | HCID 18412489 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18412535 | HCID 18412535 | 95% |
Reaction Steps
Prepared analogously to Example 26 from 1-methyl-2-[N-(4-amidinophenyl)aminomethyl]benzimidazol-5-yl-sulfonic acid-N-(1-methylpyrazol-4-yl)-N-(2-ethoxycarbonylethyl)amide hydrochloride and sodium hydroxide solution. Yield: 95% of theory, C23H26N8O4S (510.6); Rf value: 0.53 (Reversed Phase silica gel RP-18, methanol+5% saline solution); EKA mass spectrum: (M+H)+=511; (M+Na)+=533; (M+2Na)++=278.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06710055B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-f270ba826bea4201901a5c5202bcf9b8 |
| Source note | uspto-grants-2004_03 |