HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 85962067, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 10791062 | HCID 10791062 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 85962067 | HCID 85962067 | — |
Reaction Steps
Hydrolysis of 16 (10.6 g, 21.9 mmol) with 3 N KOH (40 mL) in dioxane (200 mL) at room temperature for 15 min, followed by acidification with 1 N HCl and extraction with EtOAc, gave a quantitative yield of crude 3-(bis{2-[(methylsulfonyl)oxy]ethyl}amino)-2,6-dinitrobenzoic acid (17):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07776924B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-ef93097ce9ce4c5db8f7bbf8c294893a |
| Source note | uspto-grants-2010_08 |