1-Butene → HCID 86759030, compound

HRID 503704Notes

Reaction equation

[CH2:1]=[CH:2][CH3:3].[CH3:4][CH2:5][CH:6]=[CH2:7].[CH2:8]=[CH:9][CH2:10][CH2:11][CH2:12][CH3:13]>>[CH3:7][CH2:6][CH:5]=[CH2:4].[CH2:1]=[CH:2][CH3:3].[CH2:8]=[CH:9][CH2:10][CH2:11][CH2:12][CH3:13]

Participants

Reactant 3

HCID 78441-Butene

HCID 8252Propylene3×

HCID 115971-Hexene

Product 1

HCID 86759030HCID 86759030, compound

Procedure

The preparation described in Example 13 was repeated with the difference that 5 g of propylene were fed after feeding butene-1. During polymerization the pressure was kept constant by feeding propylene. The final polymer, the characterization of which is reported in Table 1, contained 5.6% wt (NMR determination) of propylene and 4% wt of hexene. The DSC analysis showed no melting peak.

Workup

customDuring polymerization the pressure

Sources & evidence

ORD record: ord-54d7c73f4a5442428ebe425a841cffcf
Source dataset: uspto-grants-2010_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07776986B2

Reaction notes

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