Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 503745생성일: 2026년 10월 25일
4-(6-Phenylimidazo[1,2-a]pyrimidin-7-yl)benzaldehyde → 1-[4-(6-Phenylimidazo[1,2-a]pyrimidin-7-yl)phenyl]ethanol
https://huagongshe.com/reaction/503745
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 4-(6-Phenylimidazo[1,2-a]pyrimidin-7-yl)benzaldehyde | HCID 86630655 | — |
| 반응물 | HCID 178477798 | HCID 178477798 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 1-[4-(6-Phenylimidazo[1,2-a]pyrimidin-7-yl)phenyl]ethanol | HCID 68459225 | — |
반응 단계
100 mg 4-(6-phenylimidazo[1,2-a]pyrimidin-7-yl)benzaldehyde (prepared as described for example 1) are dissolved in 2 ml THF and 1 ml of a 2M solution of MeZnCl is added. The mixture is heated (100° C., microwave) for 2 h, cooled to room temperature and extracted with a mixture of dichloromethane and water. The organic layers are dried over sodium sulphate and the solvent is evaporated.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07776864B2 |
|---|
| 출처 데이터셋 | uspto-grants-2010_08 |
|---|
| ORD ID | ord-16340b00995b4d2ab54bd087e58b4918 |
|---|
| 출처 메모 | uspto-grants-2010_08 |
|---|
