HRID503781

反应详情

EQUATION

反应方程式

HRID 503781 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To 8.79 g 2-methyl-6-phenyl-5-(4-{[4-(5-pyridin-2-yl-1H-1,2,4-triazol-3-yl)piperidin-1-yl]methyl}phenyl)[1,2,4]triazolo[1,5-a]pyrimidine (prepared as described under example 37) in 88 ml methanol are added 2.85 ml hydrochloric acid solution (5.84N in methanol). The mixture is stirred at room temperature for 1 h. The solvent is removed to yield the desired product.

WORKUP

后处理

  1. customThe solvent is removed