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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 50389Generated: November 2, 2026

HCID 140409624, compound → HCID 140409614, compound

https://huagongshe.com/reaction/50389

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 140409624HCID 140409624—
SolventDichloromethane ethanolHCID 21584144—
ProductHCID 140409614HCID 14040961426%

Reaction Steps

Prepared analogously to Example 165 from 1-methyl-2-[N-[4-(N-n-hexyloxycarbonylamidino)phenyl]aminomethyl]benzimidazol-5-yl-carboxylic acid-N-phenyl-N-(3-benzyloxy-n-propyl)amide by catalytic debenzylation. Yield: 26% of theory, C33H40N6O4 (584.7); Rf value: 0.39 (silica gel; dichloromethane/ethanol=9:1); EKA mass spectrum: (M+H)+=585; (M+H+Na)++=304; (M+Na)+=607.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06710055B2
Source datasetuspto-grants-2004_03
ORD IDord-d4a6d00089214e86860bb24c81308b39
Source noteuspto-grants-2004_03