HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 140409624, compound → HCID 140409614, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 140409624 | HCID 140409624 | — |
| Solvent | Dichloromethane ethanol | HCID 21584144 | — |
| Product | HCID 140409614 | HCID 140409614 | 26% |
Reaction Steps
Prepared analogously to Example 165 from 1-methyl-2-[N-[4-(N-n-hexyloxycarbonylamidino)phenyl]aminomethyl]benzimidazol-5-yl-carboxylic acid-N-phenyl-N-(3-benzyloxy-n-propyl)amide by catalytic debenzylation. Yield: 26% of theory, C33H40N6O4 (584.7); Rf value: 0.39 (silica gel; dichloromethane/ethanol=9:1); EKA mass spectrum: (M+H)+=585; (M+H+Na)++=304; (M+Na)+=607.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06710055B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-d4a6d00089214e86860bb24c81308b39 |
| Source note | uspto-grants-2004_03 |