HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 59428371, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 66877038 | HCID 66877038 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 59428371 | HCID 59428371 | — |
Reaction Steps
3-[4-(3-Fluoro-benzenesulfonyl)-2-methylcarbamoylmethoxy-phenyl]-pyrrolidine-1-carboxylic acid tert-butyl ester was deprotected using HCl in 1,4-dioxane following the procedure described in Example 13, to afford 2-[5-(3-Fluoro-benzenesulfonyl)-2-pyrrolidin-3-yl-phenoxy]-N-methyl-acetamide as a hydrochloride salt. MS (M+H)=393.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07776910B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-d3d56c65686f44b1b11af357bc595726 |
| Source note | uspto-grants-2010_08 |