Ammonia → HCID 131728290, compound

HRID 504086Notes

Reaction equation

HRID 504086 reaction equation
[OH-].[Na+].Cl.[C:4]([O:8][CH:9]([C:11]([O:14][CH2:15][C:16]([C:19]([OH:21])=[O:20])([F:18])[F:17])([F:13])[F:12])[F:10])([F:7])([F:6])[F:5].[NH3:22]>>[C:4]([O:8][CH:9]([C:11]([O:14][CH2:15][C:16]([C:19]([O-:21])=[O:20])([F:18])[F:17])([F:12])[F:13])[F:10])([F:7])([F:6])[F:5].[NH4+:22]

Participants

5

Reactant 4

HCID 222AmmoniaHCID 313Hydrochloric AcidHCID 14798Sodium HydroxideHCID 131728291HCID 131728291, compound

Product 1

HCID 131728290HCID 131728290, compound

Procedure

This mixture was subjected to hydrolysis with a 6 N aqueous solution of sodium hydroxide, and the hydrolysis product was lyophilized and then neutralized with 12 N hydrochloric acid. The thus-obtained CF3OCHFCF2OCH2CF2COOH was neutralized with aqueous ammonia and the neutralization product was lyophilized to give 45.7 g of CF3OCHFCF2OCH2CF2COONH4.

Sources & evidence

ORD record
ord-0fb4b8aef70047cdbab0438c0358cb27
Source dataset
uspto-grants-2010_08
Patent number
US07777075B2

Reaction notes

Loading…