反应详情

Into a 1000 ml high-pressure reaction vessel add 200 g 3,4,5-Trichlorobenzotrifluoride and 145 g water, enclose the reaction vessel, fill liquid ammonia 380 g, close the valve, start agitation, slowly increase temperature to 160° C. and pressure to 10.0 MPa, make timed temperature-retention under controlled temperature 165° C. and controlled pressure 11.5 MPa for 8 h, then release the pressure and discharge ammonia.

1. customInto a 1000 ml high-pressure reaction vessel
2. customclose the valve
3. customto 160° C.
4. customunder controlled temperature 165° C. and controlled pressure 11.5 MPa
5. customfor 8 h