Hydrazine hydrate (1:1) → HCID 59428939, compound

Participants

Reaction Steps

A mixture of the compound obtained in step d) (0.183 g, 0.382 mmol) in EtOH (20 cm3) and of FeO(OH) as catalyst (20 mg) was heated to 60° C. under N2 atmosphere. Then hydrazine hydrate (19.5 mg, 0.60 mmol) was added and the resulting mixture was stirred 18 h at RT. After filtration through celite the solvent was removed at the rotary evaporator to yield a yellow oil which was dried under reduced pressure. (0.112 g, 0.248 mmol, yield 65.0%).

Provenance & Evidence