HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 61504782, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 66744398 | HCID 66744398 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 61504782 | HCID 61504782 | — |
Reaction Steps
A solution of 4-(2-methoxymethyl-phenyl)-piperazine-1-carboxylic acid tert-butyl ester (prepared as described herein below) in dioxan was treated with 4 eq. of 4M HCl in dioxane and stirred at RT for 16 h. After neutralization, the mixture was completely evaporated to give the crude title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07781436B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-e887fee0ffaa46aabd84644a9bdff2b3 |
| Source note | uspto-grants-2010_08 |