HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178503342, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 86608957 | HCID 86608957 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 178503342 | HCID 178503342 | 94% |
Reaction Steps
Methyl iodide (0.30 ml, 4.86 mmol) was added to a suspension of 6-chloro-4-methyl-3,4-dihydro-1H-quinazoline-2-thione (345 mg, 1.62 mmol) in acetone (4.8 ml). The mixture was stirred for 2 hours (r.t.), diluted with diethyl ether and the title compound (538 mg, 94%) was isolated from the reaction mixture by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07781441B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-fe297195786f4c99aad836d48acca15c |
| Source note | uspto-grants-2010_08 |