HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 11371655, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 11255888 | HCID 11255888 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 11371655 | HCID 11371655 | — |
Reaction Steps
The acid chloride of 11 (80 mg, 0.mmol mmol) was added to a solution of excess dimethylamine in dichloroethane containing a catalytic amount of DMAP at room temperature. After stirring for 30 min the reaction mixture was washed with 1M HCl then brine. Drying (Na2SO4) and concentration gave the amide 12.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07781457B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-e9a7012afe254fd5aec6ca9187b69441 |
| Source note | uspto-grants-2010_08 |