HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 59430736, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 59430737 | HCID 59430737 | — |
| Product | HCID 59430736 | HCID 59430736 | — |
Reaction Steps
To the compound of Example 1-2 (384 mg, 0.92 mmol) was added sodium hydroxide in methanol (0.1 mol/l, 9.2 ml, 0.92 mmol) and the solvent was removed in vacuo. The residue was subjected to azeotropic distillation with diethyl ether to give the subject compound (quant.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07781479B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-6ec837cfa431425bbb09b9526f024122 |
| Source note | uspto-grants-2010_08 |