Lithium Hydroxide → HCID 178509970, compound

Participants

Reaction Steps

1.0 g (2.3 mmol) of the compound from Example 32 was dissolved in 100 ml of water and admixed with 0.56 g (23.4 mmol) of lithium hydroxide, dissolved in 20 ml of water. The entire mixture was stirred at room temperature for 90 minutes. The organic solvent was subsequently removed under reduced pressure and the resulting aqueous phase was neutralized carefully using dilute hydrochloric acid. The resulting precipitate was filtered off with suction. This gave 0.55 g of the product.

Provenance & Evidence