HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Bicarbonate → HCID 178526056, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Bicarbonate | HCID 516893 | — |
| Reactant | HCID 13530948 | HCID 13530948 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 178526056 | HCID 178526056 | — |
Reaction Steps
FSO2(CF2)3OCF(CF3)COF is added dropwise to a flask under cooling with ice, into which potassium bicarbonate and monoglyme are charged, with stirring. After completion of the dropwise addition, stirring is continued further for 30 minutes, and then the solvent is distilled off. Vacuum drying is further carried out to obtain FSO2(CF2)3OCF(CF3)COOK.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07781612B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-f10354bd39e84bc5aeb03cfc0e8fa19b |
| Source note | uspto-grants-2010_08 |