HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 68420889, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 57659801 | HCID 57659801 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68420889 | HCID 68420889 | 55% |
Reaction Steps
Methyl 4-cyclopropyl-1,2,3-thiadiazole-5-carboxylate (2 g; 11 mmols) was dissolved in methanol (5 ml), and aqueous ammonia (5 ml) was added thereto, followed by stirring at room temperature for 1 hour. Subsequently, the reaction mixture was concentrated under reduced pressure, and the residue was washed with hexane to obtain 1 g of 4-cyclopropyl-1,2,3-thiadiazole-5-carboxamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07786040B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-a73c15d4c9fe432ead57a56d0e1fe1bc |
| Source note | uspto-grants-2010_08 |