HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 178474132, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 178459834 | HCID 178459834 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 178474132 | HCID 178474132 | — |
Reaction Steps
10 mg of the product from example 5-1 were dissolved in 1 ml dry pyridine and 7 μl acetyl chloride were added at room temperature. After stirring over night, the solvent was evaporated and the residue dissolved in 3 ml methanol. 1 ml conc. ammonia were added and the mixture stirred for 1 hr at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07786113B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-056109d4d495401cbc49f8702a65f332 |
| Source note | uspto-grants-2010_08 |