HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Nitrate → 3-Iodo-5-(5-methyl-pyridin-2-yl)-benzoic acid methyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Nitrate | HCID 943 | — |
| Edukt | Diiodomethane | HCID 6346 | — |
| Edukt | HCID 58326661 | HCID 58326661 | — |
| Produkt | 3-Iodo-5-(5-methyl-pyridin-2-yl)-benzoic acid methyl ester | HCID 59432579 | — |
Reaktionsschritte
5-(5-methyl-pyridin-2-yl)-benzoic acid methyl ester was treated with methylene iodide and isoamy nitrate using the procedure of step 5 of preparation 6, to afford 3-iodo-5-(5-methyl-pyridin-2-yl)-benzoic acid methyl ester, MS (M+H)=353.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07786110B2 |
| Quelldatensatz | uspto-grants-2010_08 |
| ORD ID | ord-80085afea49e4dfa89bcc857df303126 |
| Quellennotiz | uspto-grants-2010_08 |