HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 68470556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 68468046 | HCID 68468046 | — |
| Product | HCID 68470556 | HCID 68470556 | 98.4% |
Reaction Steps
The product is prepared by following the procedure described in example 34 stage (k), starting with 0.110 g of 5,6-dimethoxy-1-methyl-3-[4-(thiophen-2-ylsulfanylmethyl)-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridin-2-yl]-1H-pyrrolo[3,2-b]pyridine instead of the cyclopropyl-[2-(5,6-dimethoxy-1-methyl-1H-pyrrolo[3,2-b]pyridin-3-yl)-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-ylmethyl]amine used in example 34 stage (k) and 0.8 cm3 of 5N potassium hydroxide. 0.080 g of 5,6-dimethoxy-1-methyl-3-[4-(thiophen-2-ylsulfanylmethyl)-1H-pyrrolo[2,3-b]pyridin-2-yl]-1H-pyrrolo[3,2-b]pyridine is obtained with the following characteristics:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07786114B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-c1a961513c4a40d2a5e7d8bcb28fa34d |
| Source note | uspto-grants-2010_08 |