HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22964513, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59432792 | HCID 59432792 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22964513 | HCID 22964513 | 135.8% |
Reaction Steps
To a solution of 4-(methyl-propyl-amino)-piperidine-1-carboxylic acid tert-butyl ester (106 mg, 0.41 mmol) in AcOEt (10 ml) was added 3N HCl (4 ml). The reaction mixture was stirred for 16 hrs at RT. The solvent was removed under reduced pressure to give the desired methyl-piperidin-4-yl-propyl-amine (87 mg, 92% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07786121B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-3b395b38d67c407eadb1c20f3c55d2a0 |
| Source note | uspto-grants-2010_08 |