HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 11542083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 11542084 | HCID 11542084 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 11542083 | HCID 11542083 | — |
Reaction Steps
Add 1.0 N HCl in ethyl ether (0.0500 mL) to a solution of (S)-(3,5-Bis-trifluoromethyl-benzyl)-(7-methyl-1-pyridin-4-ylmethyl-8-trifluoromethyl-2,3,4,5-tetrahydro-1H-benzo[b]azepin-5-yl)-(2-methyl-2H-tetrazol-5-yl)-amine (0.0230 mg, 0.0357 mmole) in ethyl ether (0.500 mL), stir for 10 minutes. Evaporate the solvent to provide the title compound. MS (ES+): 644 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07786108B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-d0dfe37f8f25430fa2e476d3d07d72ea |
| Source note | uspto-grants-2010_08 |