Hydrochloric Acid → HCID 86615664, compound

Participants

Reaction Steps

Dissolve (S)-(3,5-Bis-trifluoromethyl-benzyl)-(1-cyclopropylmethyl-7,9-dimethyl-8-trifluoromethyl-2,3,4,5-tetrahydro-1H-benzo[b]azepin-5-yl)-(2-methyl-2H-tetrazol-5-yl)-amine (Example 148) (0.0210 g, 0.0338 mmol) in ethyl ether (0.5 mL). Add HCl in ether (1.0 N, 0.0338 mL). Evaporate the solvent and then triturate the residue with hexane to provide an off-white powder. MS (ES+): 621 (M+H).

Provenance & Evidence