HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86615671, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 11621361 | HCID 11621361 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86615671 | HCID 86615671 | — |
Reaction Steps
To a solution of (S)-(3,5-Bis-trifluoromethyl-benzyl)-(2-methyl-2H-tetrazol-5-yl)-(5-pyridin-4-ylmethyl-3,5,6,7,8,9-hexahydro-1H-2-oxa-5-aza-cyclohepta[f]inden-9-yl)-amine (Example 103) in diethyl ethyl ether, add HCl as a 1.0 M solution in diethyl ether. Remove solvent under a slow stream of nitrogen followed by vacuum to obtain the title compound as an off white solid. MS (ES+): 580 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07786108B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-a8e1b9fc94bc4cd2ae29bf59264aaae7 |
| Source note | uspto-grants-2010_08 |