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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 507168Generated: November 1, 2026

Hydrochloric Acid → HCID 86615671, compound

https://huagongshe.com/reaction/507168

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 11621361HCID 11621361—
SolventDiethyl EtherHCID 3283—
ProductHCID 86615671HCID 86615671—

Reaction Steps

To a solution of (S)-(3,5-Bis-trifluoromethyl-benzyl)-(2-methyl-2H-tetrazol-5-yl)-(5-pyridin-4-ylmethyl-3,5,6,7,8,9-hexahydro-1H-2-oxa-5-aza-cyclohepta[f]inden-9-yl)-amine (Example 103) in diethyl ethyl ether, add HCl as a 1.0 M solution in diethyl ether. Remove solvent under a slow stream of nitrogen followed by vacuum to obtain the title compound as an off white solid. MS (ES+): 580 (M+H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07786108B2
Source datasetuspto-grants-2010_08
ORD IDord-a8e1b9fc94bc4cd2ae29bf59264aaae7
Source noteuspto-grants-2010_08