HCID 66775446, compound → HCID 58807411, compound

HRID 507894Notes

Reaction equation

HRID 507894 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([F:15])[C:5]([CH:9]=[CH:10][C@H:11]([CH3:14])[CH2:12][CH3:13])=[C:6]([F:8])[CH:7]=1>CCCCCCC.[Pt]>[Br:1][C:2]1[CH:7]=[C:6]([F:8])[C:5]([CH2:9][CH2:10][C@H:11]([CH3:14])[CH2:12][CH3:13])=[C:4]([F:15])[CH:3]=1

Participants

4

Reactant 1

HCID 66775446HCID 66775446, compound

Product 1

HCID 58807411HCID 58807411, compound

Reagents, catalysts & solvents 2

HCID 23939PlatinumCatalystHCID 8900HeptaneSolvent

Procedure

0.4 g of 5% Pt/C (dry) is added to a solution of 1.8 g (5.9 mmol) of 2 in 50 ml of heptane, and the mixture is hydrogenated at atmospheric pressure for 20 hours. The solvent is removed under reduced pressure, and the entire amount is converted into 4.

Workup

  1. customThe solvent is removed under reduced pressure

Sources & evidence

ORD record
ord-2c8b9aaa59904d3f9fa0dbc84af6f88a
Source dataset
uspto-grants-2010_08
Patent number
US07786332B2

Reaction notes

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