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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 508017Generated: October 28, 2026

Ethyl 6-(acetylamino)-4'-(benzyloxy)-2',6'-dimethylbiphenyl-3-carboxylate → HCID 23157389, compound

https://huagongshe.com/reaction/508017

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthyl 6-(acetylamino)-4'-(benzyloxy)-2',6'-dimethylbiphenyl-3-carboxylateHCID 23157386—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 23157389HCID 2315738986%

Reaction Steps

A mixture of ethyl 6-(acetylamino)-4′-(benzyloxy)-2′,6′-dimethylbiphenyl-3-carboxylate (809 mg, 1.94 mmol), 10% palladium-carbon (50% water-containing product, 404 mg) and ethanol (10 mL) was stirred overnight under a hydrogen atmosphere at room temperature. The catalyst was filtered off, and the filtrate was concentrated under reduced pressure to give the title compound (544 mg, yield 86%) as colorless crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07786165B2
Source datasetuspto-grants-2010_08
ORD IDord-1e2601321a1a46dbb5ae559a80275a86
Source noteuspto-grants-2010_08