HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 6-(acetylamino)-4'-(benzyloxy)-2',6'-dimethylbiphenyl-3-carboxylate → HCID 23157389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 6-(acetylamino)-4'-(benzyloxy)-2',6'-dimethylbiphenyl-3-carboxylate | HCID 23157386 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23157389 | HCID 23157389 | 86% |
Reaction Steps
A mixture of ethyl 6-(acetylamino)-4′-(benzyloxy)-2′,6′-dimethylbiphenyl-3-carboxylate (809 mg, 1.94 mmol), 10% palladium-carbon (50% water-containing product, 404 mg) and ethanol (10 mL) was stirred overnight under a hydrogen atmosphere at room temperature. The catalyst was filtered off, and the filtrate was concentrated under reduced pressure to give the title compound (544 mg, yield 86%) as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07786165B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-1e2601321a1a46dbb5ae559a80275a86 |
| Source note | uspto-grants-2010_08 |