HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 86624378, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 23157445 | HCID 23157445 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86624378 | HCID 86624378 | 83.4% |
Reaction Steps
To a solution of 3-[6-({[4′-(2-ethoxyethoxy)-2′,6′-dimethylbiphenyl-3-yl]methyl}amino)pyridin-3-yl]propanoic acid (0.729 g, 1.63 mmol) in diethyl ether (5 mL) and ethyl acetate (5 mL) was added methanesulfonic acid (0.157 g, 1.63 mmol), and the resulting crystals were washed with diethyl ether to give the title compound (0.740 g, yield 83%) as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07786165B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-bdfbaac1539b4025a3bc77a45e348583 |
| Source note | uspto-grants-2010_08 |