HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 86624383, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 23157261 | HCID 23157261 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86624383 | HCID 86624383 | 73% |
Reaction Steps
3-[4-({[2′,6′-Dimethyl-4′-(2-morpholin-4-ylethoxy)biphenyl-3-yl]methyl}amino)-2-fluorophenyl]propanoic acid (0.58 g, 1.14 mmol) was dissolved in ethyl acetate (5 mL), and methanesulfonic acid (0.08 mL) was added. The precipitated crystals were collected by filtration, washed, and dried to give the title compound as colorless crystals. yield 73%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07786165B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-508d906953e448d5a5b0c975cc719739 |
| Source note | uspto-grants-2010_08 |