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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 508077Generated: November 2, 2026

Methanesulfonic Acid → HCID 86624383, compound

https://huagongshe.com/reaction/508077

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanesulfonic AcidHCID 6395—
ReactantHCID 23157261HCID 23157261—
SolventEthyl AcetateHCID 8857—
ProductHCID 86624383HCID 8662438373%

Reaction Steps

3-[4-({[2′,6′-Dimethyl-4′-(2-morpholin-4-ylethoxy)biphenyl-3-yl]methyl}amino)-2-fluorophenyl]propanoic acid (0.58 g, 1.14 mmol) was dissolved in ethyl acetate (5 mL), and methanesulfonic acid (0.08 mL) was added. The precipitated crystals were collected by filtration, washed, and dried to give the title compound as colorless crystals. yield 73%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07786165B2
Source datasetuspto-grants-2010_08
ORD IDord-508d906953e448d5a5b0c975cc719739
Source noteuspto-grants-2010_08