HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68278912, compound → HCID 68278953, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68278912 | HCID 68278912 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68278953 | HCID 68278953 | — |
Reaction Steps
To a solution of methyl 4-(benzyloxy)-2-(prop-1-en-2-yl)benzoate (i-1d) (4.6 g, 16.3 mmol) in methanol (100 ml) was added Pd/C (0.46 g). The mixture was stirred at rt under H2 atmosphere for 24 h. Then the mixture was filtered, and the filtrate was concentrated to afford the title compound. LCMS (ESI) calc'd for C11H14O3 [M+H]+: 195.1. found: 195.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09095583B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-1c5a44644fbd456bb94fb401d6c5abfa |
| Source note | uspto-grants-2015_08 |