HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11222461, compound → HCID 52951615, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11222461 | HCID 11222461 | — |
| Reactant | HCID 12082818 | HCID 12082818 | — |
| Product | HCID 52951615 | HCID 52951615 | 65% |
Reaction Steps
The titled compound was prepared in 65% yield from the compound 3a using the procedure detailed for compound 12b. mp 133.0-135.5° C. 1H NMR (300 MHz, DMSO-d6): δ 10.03 (s, 1H), 8.02 (d, J=9 Hz, 2H), 7.63 (d, J=9 Hz, 2H), 7.47-7.39 (m, 3H), 7.37-7.29 (m, 2H), 7.22 (s, 1H), 3.29 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09096532B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-fe75426ddf3749f48fd69dfcd06c738c |
| Source note | uspto-grants-2015_08 |