HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Oxalyl chloride → 3-Fluoro-4-iodobenzoyl isocyanate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Oxalyl chloride | HCID 65578 | — |
| Edukt | 3-Fluoro-4-iodobenzamide | HCID 53583829 | — |
| Lösungsmittel | 1,2-Dichloroethane | HCID 11 | — |
| Produkt | 3-Fluoro-4-iodobenzoyl isocyanate | HCID 90019121 | — |
Reaktionsschritte
The title compound was prepared according to the procedure described in step-2 of Intermediate-8 by using 3-fluoro-4-iodobenzamide (2.0 g), oxalyl chloride (0.120 mL) and EDC (25 mL) to afford 1.0 g of the desired product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09096545B2 |
| Quelldatensatz | uspto-grants-2015_08 |
| ORD ID | ord-494a9dc3530b49688d48cf5fce3ab2ad |
| Quellennotiz | uspto-grants-2015_08 |