HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 57779708, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 57779521 | HCID 57779521 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57779708 | HCID 57779708 | 99% |
Reaction Steps
Following the same procedure as described in Example 10, step 1, but substituting 2-nitro-4-(thiophen-2-yl)aniline for compound 91, and MeOH for EtOH, the title compound 92 (0.384 g, 99%) was obtained as a colorless oil. LRMS (ESI): (calc) 233.31 (found) 234.14 (MH)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09096565B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-61eca603e397404693d67e1e73245167 |
| Source note | uspto-grants-2015_08 |