反应详情

2-methyl-4-nitrobenzamide (E111) was dissolved in EtOH under Ar and 10% Pd/C added. The reaction was pump-purged with H2 and left stirring at room temperature overnight. The catalyst was removed by filtration and the reaction concentrated to give pure 4-amino-2-methylbenzamide (E112).

1. additionadded
2. customThe reaction was pump-purged with H2
3. waitleft
4. customThe catalyst was removed by filtration
5. concentrationthe reaction concentrated