Potassium tert-butoxide → HCID 72188192, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 1.6 g 4.6, 2.2 g 7.12 and 2.5 g potassium tert-butoxide in 30 ml N,N-dimethylformamide was stirred at 150° C. for 1.5 h under microwave irradiation. The reaction mixture was concentrated in vacuo and the resulting residue was purified by flash chromatography (dichloromethane/methanol 100:0→90:10) to give intermediate 10.1/Example 15.

Provenance & Evidence