Hydrazine, (4-chlorophenyl)-, hydrochloride (1:1) → HCID 57876045, compound

HRID 509753Notes

Reaction equation

HRID 509753 reaction equation
Br[CH2:2][CH2:3][N:4]1[CH2:8][CH2:7][CH:6]([CH3:9])[CH2:5]1.Cl.[Cl:11][C:12]1[CH:17]=[CH:16][C:15]([NH:18]N)=[CH:14][CH:13]=1.[CH3:20][N:21]1[CH2:26][CH2:25][C:24](=O)[CH2:23][CH2:22]1>C(N(CC)CC)C>[Cl:11][C:12]1[CH:17]=[CH:16][C:15]2[N:18]([CH2:2][CH2:3][N:4]3[CH2:8][CH2:7][CH:6]([CH3:9])[CH2:5]3)[C:24]3[CH2:25][CH2:26][N:21]([CH3:20])[CH2:22][C:23]=3[C:14]=2[CH:13]=1

Participants

5

Reactant 3

HCID 71600Hydrazine, (4-chlorophenyl)-, hydrochloride (1:1)HCID 740491-Methyl-4-piperidoneHCID 61288771HCID 61288771, compound

Product 1

HCID 57876045HCID 57876045, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The title compound is prepared by following Method 8 by using 1-(2-bromoethyl)-3-methylpyrrolidine, 4-chlorophenylhydrazine hydrochloride, triethylamine and N-methyl-4-piperidone

Sources & evidence

ORD record
ord-9cdd38d7f10c44ce8833400d5a4f6273
Source dataset
uspto-grants-2015_08
Patent number
US09096591B2

Reaction notes

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