Hydrochloric Acid → HCID 117856224, compound

Participants

Reaction Steps

3-tert-butoxycarbonylamino-1,1-bis-[3-(4-methoxycarbonyl-phenyl)-propyl]-piperidinium trifluoroacetate (200 mg, 0.3 mmol) is dissolved in dioxane (10 ml), a 4 M solution of HCl in dioxane (10 ml, 40 mmol) is added, stirred at room temperature overnight and concentrated in vacuo. LC (method F): tR=1.49 min; Mass spectrum (ESI+): m/z=453 [M]+.

Provenance & Evidence