Hydrochloric Acid → HCID 117856407, compound

Participants

Reaction Steps

3-tert-Butoxycarbonylamino-1-[3-(4-methoxycarbonyl-phenyl)-propyl]-1-[3-(4-methoxy-phenyl)propyl]-piperidinium trifluoroacetate (525 mg, 0.82 mmol) is dissolved in dioxane (10 ml), a 4 M solution of HCl in dioxane (10 ml, 40 mmol) is added, stirred at room temperature for 2 h and concentrated in vacuo. LC (method 004_CC_ZQ7): tR=1.80 min; Mass spectrum (ESI+): m/z=425 [M]+.

Provenance & Evidence