HCID 86720053, compound → HCID 66613791, compound

Participants

Reaction Steps

330 mg (0.57 mmol) of the compound from example 116 were initially charged in dimethylformamide (10.0 ml), then 66 mg of palladium (10% w/w on charcoal) were added and the mixture was hydrogenated at standard hydrogen pressure for two days. Subsequently, another 66 mg of palladium (10% w/w on charcoal) were added and hydrogenation was continued overnight.

Provenance & Evidence