HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid monohydrate → HCID 86664939, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | HCID 49818931 | HCID 49818931 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86664939 | HCID 86664939 | — |
Reaction Steps
200 mg of (6R,7R)-7-amino-3[E-(R)-1′-(5-methyl-2-oxo-[1,3]-dioxol-4-ylmethoxycarbonyl)-2-oxo-[1,3′]bipyrrolidinyl-3-ylidenemethyl]-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid were dissolved in 3 ml of methanol with addition of 95 mg of p-toluenesulfonic acid monohydrate and precipitated by the addition of 12 ml of isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09096610B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-4a4fa88e45754ba6bab54d96285db779 |
| Source note | uspto-grants-2015_08 |