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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 510328Generated: October 30, 2026

p-Toluenesulfonic acid monohydrate → HCID 86664939, compound

https://huagongshe.com/reaction/510328

Reaction equation

Participants

RoleNameHCIDCharge
Reactantp-Toluenesulfonic acid monohydrateHCID 521998—
ReactantHCID 49818931HCID 49818931—
SolventMethanolHCID 887—
ProductHCID 86664939HCID 86664939—

Reaction Steps

200 mg of (6R,7R)-7-amino-3[E-(R)-1′-(5-methyl-2-oxo-[1,3]-dioxol-4-ylmethoxycarbonyl)-2-oxo-[1,3′]bipyrrolidinyl-3-ylidenemethyl]-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid were dissolved in 3 ml of methanol with addition of 95 mg of p-toluenesulfonic acid monohydrate and precipitated by the addition of 12 ml of isopropanol.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09096610B2
Source datasetuspto-grants-2015_08
ORD IDord-4a4fa88e45754ba6bab54d96285db779
Source noteuspto-grants-2015_08